建立

NSDictionary *dict = [[NSDictionary alloc] initWithObjectsAndKeys:@"value1", @"key1", @"value2", @"key2", nil];

或

NSArray *keys = [NSArray arrayWithObjects:@"key1", @"key2", nil];
NSArray *objects = [NSArray arrayWithObjects:@"value1", @"value2", nil];
NSDictionary *dictionary = [NSDictionary dictionaryWithObjects:objects 
                                                       forKeys:keys];

或使用適當的文字語法

NSDictionary *dict = @{@"key": @"value", @"nextKey": @"nextValue"};